Prima Yudha S. Sal, Morina Adfa, Swadexi Istiqphara, Muhamad Alvin Reagen, Teja Dwi Sutanto
Cobalt nitrate solution is combined with oil palm leaf powder to produce a semisolid mixture. The resulting mixture is heated in a furnace at 500 °C for 5 h, producing a grey powder. X-ray diffraction (XRD) analysis of the product showed distinct peaks at 2θ values of 31.2°, 36.8°, 44.8°, 59.2°, and 65.1°, which were consistent with the presence of Co₃O₄/SiO₂. When a similar mixture was heated at 1000 °C for 5 h, a purple powder containing Co₂SiO₄/SiO₂ was obtained. XRD patterns of this material contained peaks at 2θ values of 25.4°, 32.2°, 34.1°, 35.6°, 36.5°, 52.2°, and 62.3°, which corresponded with Co₂SiO₄. The latter product was selected for further analysis, including Fourier-transform infrared (FTIR) spectroscopy which identified characteristic absorption bands at 588 cm⁻¹ and 672 cm⁻¹, alongside additional peaks at 817 cm⁻¹ and 1117 cm⁻¹, reflecting the formation of cobalt silicate. Energy-dispersive X-ray (EDX) analysis confirmed the presence of cobalt (20.7%), silicon (14.0%), and oxygen (45.5%), alongside minor quantities of other elements, while scanning electron microscopy (SEM) showed irregularly shaped, non-spherical particles with some aggregation and a cloudy network. Following characterization, the synthesized cobalt silicate was applied as a colorant in natural rubber latex. Preliminary observations suggest that it functioned effectively as a colorant and remains stable during extended storage. © 2026, Universitas Jenderal Soedirman. All rights reserved.
Department of Chemistry, Faculty of Mathematics and Natural Sciences, Universitas Bengkulu, Kandang Limun, Kota Bengkulu, 38122, Indonesia; Department of electrical engineering, Institut Teknologi Sumatera (ITERA), Kecamatan Jati Agung, Kabupaten Lampung Selatan, Lampung, Indonesia
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